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Accept and continue Learn more about the cookies we use and how to change your settings. Amplifies the general principles to be observed in designing experiments for the numerical estimation of the precision of measurement methods by means of a collaborative interlaboratory experiment, provides a detailed practical description of the basic method for routine use in estimating the precision of measurement methods, provides guidance to all personnel concerned with designing, performing or analysing the results of the tests for estimating precision.
Analytical results as percentage Mn Lab. Intermediate measures of the precision of a standard measurement method – Part 4: Here B is the laboratory component of bias, i. General principles and definitions – Part 2: Prior to conducting the as- sessment of trueness, a ios of the precision of the standard measurement method as applied by the lab- oratory shall be performed.
BS ISO 5725-2:1994
What action is to be taken concerning its publication? The purpose of the two-bottle system was to confirm the absence of the between-bottle variation.
Therefore the Index j for the level has been omitted throughout. In this report the following information shall be given: In chemical anal- ysis, problems may arise from, for example, insufficient control of temperature, moisture, pres- ence of contaminants, etc.
ISO Accuracy of measurement methods and results-Part 2 Basic method – MBA智库文档
IS0 l should be read in conjunction with all other parts of IS0 57725-2, including this part, because it gives the underlying definitions and general principles.
It was therefore decided to discard the results from laboratory 10 completely; it should be the object of special attention, and the matter should be resolved. If u, is un- known, its estimate s.
All measurements are to be carried out according to that standard method. Basic methods for the determination of the trueness of a standard measurement method 1 Scope 1. When gR is larger than T. The reference material should have a matrix as close as possible to the matrix of the material to be subjected to 525-2 standard measurement method, e.
There again, appropriate action should be taken by investigating these laboratories, or, if necessary, by tightening the protocol of the measurement method.
Apart from the restriction to a single laboratory. The test results for each level are shown in figures B.
Please proceed with checkout. Basic method for the determination of repeatability and re- producibility of a standard measurement method – Part 3: Isi materials could be either a certified reference materials; b materials manufactured for the purpose sio the experiment with known properties; or c materials whose properties have been established by measurements using an alternative measure- ment method whose bias is known to be negligi- ble. Unless otherwise stated, a is assumed to be 0, Unless otherwise stated, a is assumed to be 0.
Bias can arise, for example, in 575-2 analysis if the measurement method fails to extract all of an element, or if the presence of one element interferes with the determination of another.
This implies comparison between the within-laboratory standard deviation and the stated repeatability standard deviation of the standard measurement method.
GSO ISO – Standards Store – GCC Standardization Organization
If the repeatability of the measurement method is poor, then it will not be practical to achieve a high degree of certainty in the estimate of the bias of the laboratory.
The repeatability and the reproducibility standard de- viations were then computed excluding those data that were discarded. IS0 consists of the following parts, under the general title Accuracy trueness and precision of measurement methods and results: To request this FREE document, please email us. It is not applicable if the bias in the measurement of one property is affected by the level of a second property i. In the former case, the repeatability standard devi- ation of the measurement method, or, will be used for the assessment of the laboratory bias.
Annex B provides practical examples of estimating the precision of measurement methods by experiment. Alternative methods for the determination of the precision of a standard measurement method – Part 6: Relevant International Standards on sample division should isp consulted. Do the results of the accuracy experiment justify the acceptability of the measurement method for adoption as a standard?
Ministry of 5752-2 and Industry.
Trueness is normally expressed in terms of bias. The analytical results are listed in tableB. It may appear that some laboratories did not use the required equipment or did not work ac- cording to the specified conditions.
Company organization, management and quality. The k values figure B-7 show that laboratories Specifies four intermediate measures due to changes in observation conditions time, calibration, operator and equipment within a laboratory.